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    High-pressure Quartz Crystal Microbalance

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    8718956.pdf (907.9Kb)
    Date
    5/6/2014
    Author
    Hesketh, Peter
    Nair, Sankar
    Mccarley, Ken
    Navaei, Milad
    Bagnall, Kevin
    Venkatasubramanian, Anandram
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    Abstract
    Described is an apparatus for measuring mass change under high pressure, comprising: a high pressure cell comprising a reference quartz crystal microbalance sensor and a sample quartz crystal microbalance sensor, wherein the sample quartz crystal microbalance sensor is coated with a test sample selected from the group consisting of nanoporous materials and metal-organic frameworks; a pressure sensor operatively connected to the high pressure cell; a thermocouple operatively connected to the high pressure cell, wherein the high pressure cell is maintained at a pre-selected temperature; a gas inlet fluidly connected to the high pressure cell; and a gas outlet fluidly connected to the high pressure cell. Also described are methods of making and using the apparatus.
    URI
    http://hdl.handle.net/1853/56881
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